Empyrean PANalytical X-Ray Diffractometer

Applications: X-ray phase analysis of macro-, micro-, nanocrystallite and amorphous materials, thin films, powders, solid objects.

Research possibilities:

  • qualitative phase analysis;
  • quantitative phase analysis;
  • measurements of texture;
  • residual stress analysis;
  • Rietveld analysis;
  • temperature measurements.
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Equipment:

  • ceramic X-ray tube (anode materials: Cu, Co, Mo);
  • detectors: PIXcel3D & proportional detector;
  • high-temperature chamber Anton Paar HTK 16N for in-situ diffraction studies in high temperatures up to 1600ºC;
  • high-temperature chamber Anton Paar HTK 2000N with temperature range of 25–2300°C.

Four kinds of sample stages:

  • stationary sample stage for measuring flat samples;
  • reflection-transmission spinner with the option of rotating the samples (powders and solid objects);
  • 3-axis (Chi-Phi-Z) cradle for measuring residual stress and sample texture;
  • 5-axis (Chi-Phi-XYZ) cradle for measuring reflectivity, residual stress and sample texture.

Software:

  • HighScore Plus;
  • Stress Plus;
  • Texture;
  • PDF-4+ (ICDD) – diffraction database.

Location: Centre of Materials Research at Łukasiewicz Research Network – Krakow Institute of Technology.
See CV of the responsible person.
See address of the Centre of Materials Research at LRN-KIT

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X-Ray based Technique

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